Cold process procedure.
Note: all
measurements are by weight, not by volume. A digital scale set to
ounces is the most effective, for the lye measurements must be
precise.
Prepare the lye.
Using a lye
calculator, which can be found on the internet, learn how much lye
and water will be needed for the recipe. Weigh the correct amount
of water in a container that will never be used for any other
purpose and gently pour the lye into the water. Stir the solution
until all lye is dissolved. Lye is caustic, so here is my list of
don'ts:
Do not pour the water into the lye, the resulting
chemical reaction is a little lye volcano.
Do not let the mixture
splash. Gentle. Be gentle.
Do not let yourself get interrupted
during this step.
The chemical reaction will cause the water to
heat above 200 degrees. Set aside to cool.
Prepare the fats.
Continue to
consult the lye calculator.
In a pan, (which can still be used
for other purposes afterwards) heat the solid fats first, allowing
them to liquify, then add the liquid fats.
Allow the fats and the lye to come
to the same temperature.
This is a matter of preference or
recipe instructions. Around 100 degrees is a good rule-of-thumb for
the goal temperature. Plant-based fats can be lower, animal-based
fats can be higher. The oils or the lye can be reheated if one has
cooled too much to combine with the other, or cooled by placing the
container in a tub of cold water.
Combine.
When the two
substances are at the same temperature, slowly pour the lye into the
oils.
Stir the mixture constantly, do not allow yourself to be
interrupted during this process, and continue stirring until a trace
is reached.
A trace is reached when the solution has a
pudding-like consistency, so that when the spoon or stick blender is
pulled out of the mixture, the drippings leave an impression on the
surface of the mixture.
At this point, stir in any
additives that you were planning on using.
Pour the soap into the mold or
molds.
Cover them with a lid or a sheet of cardboard. Insulate
the molds by wrapping them in 3 or 4 towels. Store the molds in a
moderately warm place for about 24 hours.
Let cure.
Remove the soap from
the molds after about a day. If you used a loaf mold, cut the soap
into smaller pieces. Lay the soap upright on a piece of cardboard
or a drying rack – good airflow is the goal. Place somewhere where
it will not be disturbed and let finish curing – 4 weeks unless
the recipe says otherwise. For good circulation, you may wish to
flip the soap every week or so. After the appropriate time, the
soap is ready for use.
Tip: In some cases, a white residue
may form on your soap. Brush this off before use.
Measure your additives before you combine the lye mixture with the oils.
Sometimes the
soaps reach their trace and begin to harden sooner than the maker is
ready, and using additives is no longer possible. The batch is not
lost. Allow the soap to set for a day, then see the instructions for
milling soap.
Hot process
soap procedure
Note: all measurements are by weight,
not by volume. A digital scale set to ounces is the most effective,
for the lye measurements must be precise.
Prepare the lye.
Using a lye
calculator, which can be found on the internet, learn how much lye
and water will be needed for the recipe. Weigh the correct amount
of water in a container that will never be used for any other
purpose and gently pour the lye into the water while stirring the
water. Keep stirring the solution until all lye is dissolved. Lye
is caustic, so here is my list of don'ts:
Do not pour the water
into the lye, the resulting chemical reaction is a little lye
volcano.
Do not let the mixture splash. Gentle. Be gentle.
Do
not let yourself get interrupted during this step.
The chemical
reaction will cause the water to heat above 200 degrees. Set aside
to cool.
Prepare the fats.
Continue to
consult the lye calculator. Weigh your oils and fats and place in
an active crock pot. Begin with the solids and allow them to melt
before adding the liquids.
Combine.
It is not necessary for the lye and
the fats to be the same temperature when they are combined. Slowly
add the lye water to the crock pot, stirring constantly. Do not
allow yourself to be interrupted during this process, and continue
stirring until a trace is reached.
A trace is reached when the
solution has a pudding-like consistency, so that when the spoon or
stick blender is pulled out of the mixture, the drippings leave an
impression on the surface of the mixture.
Heat.
Cover the crock pot, set it to low and
be vigilant over it. Make sure that it does not bubble over as it
cures: stir it gently if it does, it is otherwise not necessary to
disturb the mixture.
Test the batch
The mix will begin to take on a clear
Vaseline like look after about an hour. Once the whole mix has this
look, test it to see if it is done. Take a small sample of the soap
and rub it between your fingers. It should have a waxy feel. Test
the soap by touching it to your tongue, if it 'zaps' like a nine
volt battery, it's not done. Keep cooking until it no longer 'zaps'.
Additives
Turn off the crock pot and mix your
additives, waiting until the batch has cooled slightly before adding
your essential oils - if the batch is hotter than the flash point of
your oils, the oils will vaporize, fun!
Add to molds
Unlike cold process soap, hot process soap is a gelatinous mass.
Scoop it into the molds and then tap the molds against a hard surface
to let any air bubbles escape. Allow 1-2 days for the soap to harden
before removing from the molds. Cut the soap immediately after
removal if using a larger mold. Soap is ready for use.
Tip:
This soap has a more rustic look and softer texture than cold
process. Some recipes will lend themselves better to the hardness
and smoothness of cold process. In the hot process soap, you can add
fragrances that would be too sensitive to the alkaline still present
in the cold process soap.
Soaps like floating soap and whipped
soap need to be done with the cold process.
Milled Soap
process.
Prep soap
Grate the soap down
into small pieces, this can be done with just a cheese grater,
anything electronic like a food processor tends to get gummed up
after a few minutes. It is important that the soap be reduced to
little pieces, for it can be difficult to melt.
Add liquid to the
soap when you go to melt it. The liquid can be milk or tea or
water, a general rule of thumb is 2-3 ounces of liquid per pound of
soap. Newer soap will require less, older soap will require more.
If you add too much, the soap will take a long time to dry or harden
after the process.
Melt soap
Begin with a
completed bar of soap. If the soap is cold process and has not yet
cured, take steps to protect yourself from the alkaline still in the
soap.
Grate the soap and melt it in the microwave, in a double
boiler, in a crock pot, or in a boil bag. It is important that the
soap be heated without being scorched, the which purpose can be
messy and complicated.
If you decide to use the microwave to
melt the soap, microwave it in a safe bowl in 1 minute increments
and stir as you go.
If you decide to use the crock pot or double
boiler, patience is key. The author of this guide does not have
enough to have successfully used the technique.
If you decide to
use a boil bag, set a pot of water to boil, put the soap shavings in
a heat safe freezer bag and
seal it. Put that bag in another bag and seal it, drop the bag into
the boiling water, try to avoid it touching the sides of the pot and
let it boil for 40 minutes. If it has not yet melted, add a
tablespoon of liquid and let it continue to boil for another 20
minutes. Please wear heat safe gloves.
The melted soap
will have a gummy, mashed potato-like texture, or can be comparable
to vaseline.
Pour in the additives.
Once the
soap has liquified, add in any dyes, substances or fragrances. Mix
the soap as much as necessary to distribute the substances.
Pour
the milled soaps into their molds and allow them to harden. This
can take up to 48 hours. Leave the molds where they will be dry and
undisturbed. Use your judgment if the hardening seems to take even
longer.
Remove the soap from the molds.
If
you used one large mold, cut them now.
If you used a cold
process base that was not fully cured, let the soap air dry as you
would an uncured cold process soap. Otherwise, they are ready to
use as long as they are hardened.
Tips. Generally, it makes more sense
to insert any additives in your soap during the initial cure and
avoid this process altogether, however, some soap recipes need to be
made with cold process, some additives cannot be used during cold
process due to their sensitivity to the alkaline. Occasionally,
stupid happens, distraction takes place, spontaneous improvisation
becomes necessary, whatever, so it is as well to know how to mill as
not.
Be warned: using the milling process to save a batch of
soap that has gone awry IS a gamble.
Tools
The
soap making process is not necessarily one which requires complicated
or specific tools. You need the following.
A scale.
In this process,
precision is key, particularly when it comes to measuring lye. An
accurate scale is essential, a digital scale that measures ounces to
the decimal is recommended.
A thermometer.
During the cold
process, it is necessary to combine the lye with the oils and fats
while they are almost the same temperature, and a good thermometer
is necessary. Even if you are doing the hot process, though, and
choose to have essential oils, it is necessary to make sure your
batch hasn't exceeded their flash points. A candy thermometer is
great.
Other measuring
implements.
Measuring cups, spoons, plastic containers for
weighing the fats. These will never come into contact with the pure
lye, so you needn't worry about exclusive measuring implements
unless you like things organized that way.
A heat source.
You need a means
to heat the oils and fats, and during the hot process, to cook the
batch. A crock pot is specified, but you can also do your heating
in the oven, at 170-190 degrees Fahrenheit. For the cold process, a
pan on the stove will do the trick.
Two lye containers.
A little
one for weighing out the lye and a larger one for weighing the water
and adding the lye – these containers should never be used for
anything else. Lye is a very caustic substance which heats the
water to 200 degrees, don't use glass or aluminum. Plastic will be
fine.
A stirrer.
To mix the batch,
constant stirring is necessary. This can be done with a sturdy
wooden spoon, or, recommended, a stick blender.
Molds
You need containers into
which to pour your soaps while they cure. These should be sturdy,
somewhat flexible (if they are not, line them with plastic wrap
before pouring). They can be decorative, they can be plain, they
can be an old loaf pan that no one cares about. They can be
silicone, they can be plastic, they can be rinsed out half-gallon
milk cartons with the lid chopped off. Just make sure you know what
you're going to do with your soap when you take it off the heat
source.
The writer of this guide prefers silicone because they
are reusable and the soap pops out like a dream, but don't knock
yourself out trying to find them.
Protective gear
Lye is caustic,
and without lye you can't make soap. As mentioned, lye heats up to
200 degrees when it reacts to water. When it mixes with water, it
gives off fumes. Inhaling it or getting it on yourself is a
legitimate concern, and a pair of gloves and goggles, and even a
mask wouldn't go amiss. Indeed, it falls into the category of
common sense.
That said, the writer of this guide finds these
implements cumbersome and does not use them. Whether you do or not,
don't inhale the fumes and if lye splashes on you rush to the sink
and flush the affected area. Do not apply vinegar, no matter who
tells you it's a good idea. It isn't.
Do not let the
warnings about lye cripple your ability to do the task in front of
you. Respect the substance, don't fear it. Store it in a sensible
place, keep your head, wash it off if it gets on you. Unless you
panic, you'll be fine...in fact, even IF you panic, you're probably
fine. Flush the affected area with water.